Structural transformation of MoO3 nanobelts into MoS2 nanotubes

被引：14

作者：

Deepak, Francis Leonard ^{[2
]}

Mayoral, Alvaro ^{[1
]}

Yacaman, Miguel Jose ^{[1
]}

机构：

[1] Univ Texas San Antonio, Dept Phys & Astron, San Antonio, TX 78249 USA

[2] Int Iberian Nanotechnol Lab, P-4715 Braga, Portugal

来源：

APPLIED PHYSICS A-MATERIALS SCIENCE & PROCESSING | 2009年 / 96卷 / 04期

关键词：

FULLERENE-LIKE NANOPARTICLES; SIMPLE HYDROTHERMAL ROUTE; INORGANIC NANOTUBES; LARGE-SCALE; MECHANISM; NANOWIRES; NANORODS; GROWTH;

D O I：

10.1007/s00339-009-5320-1

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

The structural transformation of MoO3 nanobelts into MoS2 nanotubes using a simple sulfur source has been reported. This transformation has been extensively investigated using electron microscopic and spectroscopic techniques including scanning electron microscopy (SEM), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), electron diffraction (ED), and energy-dispersive X-ray analysis (SEM-EDAX and TEM-EDX). The method described in this report will serve as a generic route for the transformation of other oxide nanostructures into the chalcogenide nanostructures.

引用

页码：861 / 867

页数：7

共 23 条

[1] A rational route to synthesize Bi2S3 nanorods in large scale [J].

Chai, Duoli ;

Yuan, XinSong ;

Yang, BaoJun ;

Qian, Yitai .

SOLID STATE COMMUNICATIONS, 2008, 148 (9-10) :444-447

[2] Synthesis, characterization, and formation mechanism of copper sulfide-core/carbon-sheath cables by a simple hydrothermal route [J].

Chen, Guang-Yi ;

Deng, Bin ;

Cai, Guo-Bin ;

Dong, Wen-Fei ;

Zhang, Wan-Xi ;

Xu, An-Wu .

CRYSTAL GROWTH & DESIGN, 2008, 8 (07) :2137-2143

[3] Single-Crystalline Molybdenum Trioxide Nanoribbons: Photocatalytic, Photoconductive, and Electrochemical Properties [J].

Cheng, Liang ;

Shao, Mingwang ;

Wang, Xiuhua ;

Hu, Haibo .

CHEMISTRY-A EUROPEAN JOURNAL, 2009, 15 (10) :2310-2316

[4] HIGH-RATE, GAS-PHASE GROWTH OF MOS2 NESTED INORGANIC FULLERENES AND NANOTUBES [J].

FELDMAN, Y ;

WASSERMAN, E ;

SROLOVITZ, DJ ;

TENNE, R .

SCIENCE, 1995, 267 (5195) :222-225

[5] Bulk synthesis of inorganic fullerene-like MS(2) (M=Mo, W) from the respective trioxides and the reaction mechanism [J].

Feldman, Y ;

Frey, GL ;

Homyonfer, M ;

Lyakhovitskaya, V ;

Margulis, L ;

Cohen, H ;

Hodes, G ;

Hutchison, JL ;

Tenne, R .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1996, 118 (23) :5362-5367

[6] Lithium insertion and electrochromism in polycrystalline molybdenum oxide films [J].

Ferreira, FF ;

Cruz, TGS ;

Fantini, MCA ;

Tabacniks, MH ;

de Castro, SC ;

Morais, J ;

de Siervo, A ;

Landers, R ;

Gorenstein, A .

SOLID STATE IONICS, 2000, 136 :357-363

[7] PHYSICAL PROPERTIES OF LAYER STRUCTURES - OPTICAL PROPERTIES AND PHOTOCONDUCTIVITY OF THIN CRYSTALS OF MOLYBDENUM DISULPHIDE [J].

FRINDT, RF ;

YOFFE, AD .

PROCEEDINGS OF THE ROYAL SOCIETY OF LONDON SERIES A-MATHEMATICAL AND PHYSICAL SCIENCES, 1963, 273 (1352) :69-+

[8] Comparative study on MoO3 and HxMoO3 nanobelts:: Structure and electric transport [J].

Hu, Xiao Kai ;

Qian, Yi Tai ;

Song, Z. T. ;

Huang, Jia Rui ;

Cao, R. ;

Xiao, John Q. .

CHEMISTRY OF MATERIALS, 2008, 20 (04) :1527-1533

[9] One-step synthesis and assembly of copper sulfide nanoparticles to nanowires, nanotubes, and nanovesicles by a simple organic amine-assisted hydrothermal process [J].

Lu, QY ;

Gao, F ;

Zhao, DY .

NANO LETTERS, 2002, 2 (07) :725-728

[10] Study of the growth mechanism of WS2 nanotubes produced by a fluidized bed reactor [J].

Margolin, A ;

Rosentsveig, R ;

Albu-Yaron, A ;

Popovitz-Biro, R ;

Tenne, R .

JOURNAL OF MATERIALS CHEMISTRY, 2004, 14 (04) :617-624

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