Structural mechanisms of the mechanical degradation of Ti-Al-V alloys:: in situ study during annealing

被引:19
作者
Berberich, F [1 ]
Matz, W [1 ]
Richter, E [1 ]
Schell, N [1 ]
Kreissig, U [1 ]
Möller, W [1 ]
机构
[1] Rossendorf Inc, Forschungszentrum Rossendorf EV, D-01314 Dresden, Germany
关键词
Ti-6Al-4V; ion implantation; XRD; hardness;
D O I
10.1016/S0257-8972(00)00595-8
中图分类号
TB3 [工程材料学];
学科分类号
0805 [材料科学与工程]; 080502 [材料学];
摘要
The aim of this work was to investigate the structural mechanisms of the enhanced hardness of the technical alloy Ti-6Al-4V due to N+-implantation and its degeneration. Ti-6Al-4V samples were implanted with fluences (1-6) x 10(17) N+/cm(2) at 80 keV. The structural implications of the loss of hardness during annealing were studied by in situ XRD experiments with synchrotron radiation. Additional sample characterisation was performed by SEM, ERDA and Vickers hardness tests. The hardness reduction due to annealing is caused by phase transformation from TiN to Ti2N in consequence of the diffusion of nitrogen as well as by rearrangements in the alpha-Ti and beta-Ti phase of the alloy. (C) 2000 Elsevier Science S.A. All rights reserved.
引用
收藏
页码:450 / 454
页数:5
相关论文
共 13 条
[1]
Mechanical properties and structure of Ti-6Al-4V alloy implanted with different light ions [J].
Alonso, F. ;
Arizaga, A. ;
Quainton, S. ;
Ugarte, J. J. ;
Viviente, J. L. ;
Onate, J. I. .
SURFACE & COATINGS TECHNOLOGY, 1995, 74-75 (1-3) :986-992
[2]
Boyer R., 1994, Materials Properties Handbook, V1st
[3]
MODELING OF CONCENTRATION PROFILES FROM VERY HIGH-DOSE ION-IMPLANTATION [J].
BUNKER, SN ;
ARMINI, AJ .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 1989, 39 (1-4) :7-10
[4]
MEV ION-IMPLANTATION OF N INTO TI FOR SURFACE HARDENING [J].
CUI, FZ ;
VREDENBERG, AM ;
SARIS, FW .
APPLIED PHYSICS LETTERS, 1988, 53 (22) :2152-2154
[5]
*ICDD, 381420 ICDD
[6]
HIGH-TEMPERATURE NITROGEN IMPLANTATION OF TI-6AL-4V .1. MICROSTRUCTURE CHARACTERIZATION [J].
KUSTAS, FM ;
MISRA, MS ;
WEI, R ;
WILBUR, PJ ;
KNAPP, JA .
SURFACE & COATINGS TECHNOLOGY, 1992, 51 (1-3) :100-105
[7]
HIGH-TEMPERATURE NITROGEN IMPLANTATION OF TI-6AL-4V .2. TRIBOLOGICAL PROPERTIES [J].
KUSTAS, FM ;
MISRA, MS ;
WEI, R ;
WILBUR, PJ .
SURFACE & COATINGS TECHNOLOGY, 1992, 51 (1-3) :106-111
[8]
ROBL -: a CRG beamline for radiochemistry and materials research at the ESRF [J].
Matz, W ;
Schell, N ;
Bernhard, G ;
Prokert, F ;
Reich, T ;
Claussner, J ;
Oehme, W ;
Schlenk, R ;
Dienel, S ;
Funke, H ;
Eichhorn, F ;
Betzl, M ;
Pröhl, D ;
Strauch, U ;
Hüttig, G ;
Krug, H ;
Neumann, W ;
Brendler, V ;
Reichel, P ;
Denecke, MA ;
Nitsche, H .
JOURNAL OF SYNCHROTRON RADIATION, 1999, 6 :1076-1085
[9]
THE EFFECT OF ANNEALING ON THE KNOOP MICROHARDNESS OF NITROGEN IMPLANTED TI-6AL-4V ALLOY [J].
NATH, VC ;
SOOD, DK ;
MANORY, RR .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 1991, 59 :946-950
[10]
ULTRAMICROHARDNESS AND MICROSTRUCTURE OF TI-6 WT-PERCENT-AL-4 WT-PERCENT-V ALLOY NITRIDED BY ION-IMPLANTATION [J].
NATH, VC ;
SOOD, DK ;
MANORY, RR .
SURFACE & COATINGS TECHNOLOGY, 1991, 49 (1-3) :510-513