Primary study of volatiles composition of Rhodiola sachalinensis by using gas chromatography and mass spectrometry (GC/MS)

被引:10
作者
Jin, Yinzhe [1 ,2 ]
Park, Dong Wha [1 ,4 ]
Li, Xifeng [3 ]
Li, Donghao [3 ]
Row, Kyung Ho [1 ]
机构
[1] Inha Univ, Dept Chem Engn, Inchon 402751, South Korea
[2] Shanghai Ocean Univ, Coll Food Sci & Technol, Shanghai 201306, Peoples R China
[3] Yanbian Univ, Anal & Inspect Ctr, Yanji, Jilin Province, Peoples R China
[4] Inha Univ, Reg Innovat Ctr Environm Technol Thermal Plasma, Inchon 402751, South Korea
基金
中国国家自然科学基金;
关键词
Volatiles; HD; HS-LPME; Rhodiola sachalinensis; GC/MS; SOLID-PHASE MICROEXTRACTION; SUPERCRITICAL CO2 EXTRACTION; CARBON-DIOXIDE EXTRACTION; ESSENTIAL OIL; CHEMICAL-COMPOSITION; L; DISTILLATION; SALIDROSIDE; COMPONENTS; ROOTS;
D O I
10.1007/s11814-010-0170-2
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
To determine the volatile compounds in Rhodiola sachalinensis, hydro-distillation (HD) and headspace liquid-phase micro-extraction (HS-LPME) were used to extract 75 and 68 volatiles, respectively. Geraniol (24.73%), n-octanol (15.56%), and linalool (14.51%) were the most abundant essential oils detected in the HD samples, while geraniol (24.17%) and n-octanol (15.81%) were also detected at high levels in the HS-LPME samples. The main chemical classes of the essential oils were monoterpene alcohols in both the HD and HS-LPME samples at 59.02% and 37.64%, respectively. The O-heterocyclic (8.52%) and aromatic (5.92%) compounds were more abundant in the HS-LPME samples than in the HD samples.
引用
收藏
页码:1262 / 1268
页数:7
相关论文
共 28 条
[1]   Comparison of three different solid-phase microextraction fibres for analysis of essential oils in yacon (Smallanthus sonchifolius) leaves [J].
Adam, M ;
Juklová, M ;
Bajer, T ;
Eisner, A ;
Ventura, K .
JOURNAL OF CHROMATOGRAPHY A, 2005, 1084 (1-2) :2-6
[2]   Chemical composition of the essential oil of Rhodiola quadrifida from Xinjiang, China [J].
Bai, Z ;
Nan, P ;
Zhong, Y .
CHEMISTRY OF NATURAL COMPOUNDS, 2005, 41 (04) :418-419
[3]   Supercritical CO2 extraction of essential oil from yarrow [J].
Bocevska, M. ;
Sovova, H. .
JOURNAL OF SUPERCRITICAL FLUIDS, 2007, 40 (03) :360-367
[4]   Essential oils: their antibacterial properties and potential applications in foods - a review [J].
Burt, S .
INTERNATIONAL JOURNAL OF FOOD MICROBIOLOGY, 2004, 94 (03) :223-253
[5]   Comparative study of the whisky aroma profile based on headspace solid phase microextraction using different fibre coatings [J].
Camara, J. S. ;
Marques, J. C. ;
Perestrelo, R. M. ;
Rodrigues, F. ;
Oliveira, L. ;
Andrade, P. ;
Caldeira, M. .
JOURNAL OF CHROMATOGRAPHY A, 2007, 1150 (1-2) :198-207
[6]   Fast determination of paeonol in plasma by headspace solid-phase microextraction followed by gas chromatography-mass spectrometry [J].
Dong, Ling ;
Deng, Chunhui ;
Wang, Jiyao ;
Shen, Xizhong .
ANALYTICA CHIMICA ACTA, 2007, 585 (01) :76-80
[7]   Hydrodistillation-headspace solvent microextraction, a new method for analysis of the essential oil components of Lavandula angustifolia Mill. [J].
Fakhari, AR ;
Salehi, P ;
Heydari, R ;
Ebrahimi, SN ;
Haddad, PR .
JOURNAL OF CHROMATOGRAPHY A, 2005, 1098 (1-2) :14-18
[8]   Supercritical carbon dioxide extraction of volatile oil from Italian coriander seeds [J].
Grosso, C. ;
Ferraro, V. ;
Figueiredo, A. C. ;
Barroso, J. G. ;
Coelho, J. A. ;
Palavra, A. M. .
FOOD CHEMISTRY, 2008, 111 (01) :197-203
[9]   Enhancing the production of cinnamyl glycosides in compact callus aggregate cultures of Rhodiola rosea by biotransformation of cinnamyl alcohol [J].
György, Z ;
Tolonen, A ;
Pakonen, M ;
Neubauer, P ;
Hohtola, A .
PLANT SCIENCE, 2004, 166 (01) :229-236
[10]   Determination of essential oil components of Artemisia haussknechtii Boiss using simultaneous hydrodistillation static headspace liquid phase microextraction gas chromatography mass spectrometry [J].
Heravi, M. Jalali ;
Sereshti, H. .
JOURNAL OF CHROMATOGRAPHY A, 2007, 1160 (1-2) :81-89