Shape-selected synthesis of nanocrystalline SnS in different alkaline media

被引:42
作者
An, CH [1 ]
Tang, KB [1 ]
Jin, Y [1 ]
Liu, QC [1 ]
Chen, XY [1 ]
Qian, YT [1 ]
机构
[1] Univ Sci & Technol China, Dept Chem, Struct Res Lab, Anhua 230026, Peoples R China
基金
中国国家自然科学基金;
关键词
crystal morphology; nanomaterials; semiconducting materials;
D O I
10.1016/S0022-0248(03)00961-8
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
Semiconducting Tin(II) monosulfide nanowires, nanorods and nanoparticles were successfully selectively prepared using SnCl2.2H(2)O and thiourea (Tu) as the raw materials by appropriately choosing different alkaline solution as reaction media. The SnS nanowires are uniform with diameters 30-70 nm and lengths 3-10 mum, the nanorods are about several micrometers long with average width of 60-200 nm and the nanoparticles have an even diameter of about 510 nm. Compared to the previous reports, the present method is relatively simple, without using complex apparatus, and manipulated conveniently, which may be favorable for industrial application in the future. (C) 2003 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:581 / 586
页数:6
相关论文
共 34 条
[1]   Shape-controlled synthesis of colloidal platinum nanoparticles [J].
Ahmadi, TS ;
Wang, ZL ;
Green, TC ;
Henglein, A ;
ElSayed, MA .
SCIENCE, 1996, 272 (5270) :1924-1926
[2]   THE PREPARATION AND THE ELECTRICAL AND OPTICAL PROPERTIES OF SNS CRYSTALS [J].
ALBERS, W ;
HAAS, C ;
VANDERMAESEN, F .
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 1960, 15 (3-4) :306-310
[3]   Semiconductor clusters, nanocrystals, and quantum dots [J].
Alivisatos, AP .
SCIENCE, 1996, 271 (5251) :933-937
[4]   Growth of belt-like SnS crystals from ethylenediamine solution [J].
An, CH ;
Tang, KB ;
Shen, GZ ;
Wang, CR ;
Yang, Q ;
Hai, B ;
Qian, YT .
JOURNAL OF CRYSTAL GROWTH, 2002, 244 (3-4) :333-338
[5]  
Briggs D., 1983, Practical Surface Analysis by Auger and X-ray Photoelectron Spectroscopy
[6]   NEUTRON-DIFFRACTION STUDY OF THE STRUCTURAL PHASE-TRANSITION IN SNS AND SNSE [J].
CHATTOPADHYAY, T ;
PANNETIER, J ;
VONSCHNERING, HG .
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 1986, 47 (09) :879-885
[7]  
COUSTAL R, 1931, J CHIM PHYS PCB, V31, P277
[8]   PHOTOCONDUCTIVITY IN TIN SULFIDE SINGLE-CRYSTALS [J].
ELKORASHY, AM .
PHYSICA B, 1991, 168 (04) :257-267
[9]   LOW-TEMPERATURE CHEMICAL PRECIPITATION AND VAPOR-DEPOSITION OF SNXS THIN-FILMS [J].
ENGELKEN, RD ;
MCCLOUD, HE ;
LEE, C ;
SLAYTON, M ;
GHOREISHI, H .
JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 1987, 134 (11) :2696-2707
[10]   GROWTH AND CHARACTERIZATION OF ZINC-SULFIDE FILMS BY CONVERSION OF ZINC-OXIDE FILMS WITH H2S [J].
GAO, YM ;
WU, P ;
BAGLIO, J ;
DWIGHT, K ;
WOLD, A .
MATERIALS RESEARCH BULLETIN, 1989, 24 (10) :1215-1221