CO3O4 protective coatings prepared by Pulsed Injection Metal Organic Chemical Vapour Deposition

被引:47
作者
Burriel, M
García, G
Santiso, J
Hansson, AN
Linderoth, S
Figueras, A
机构
[1] CSIC, ICMAB, Lab Crystal Growth, Bellaterra 08193, Spain
[2] Riso Natl Lab, Mat Res Dept, DK-4000 Roskilde, Denmark
[3] Inst Fis, Juriquilla 76230, Queretaro, Mexico
关键词
MOCVD; cobalt oxide; deposition process; XRD; coatings;
D O I
10.1016/j.tsf.2004.07.081
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Cobalt oxide films were grown by Pulsed Injection Metal Organic Chemical Vapour Deposition (PI-MOCVD) using Co(acac)(3) (acac=acetylacetonate) precursor dissolved in toluene. The structure, morphology and growth rate of the layers deposited on silicon substrates were studied as a function of deposition temperature. Pure Co3O4 spinel structure was found for deposition temperatures ranging from 360 to 540 degreesC. The optimum experimental parameters to prepare dense layers with a high growth rate were determined and used to prepare corrosion protective coatings for Fe-22Cr metallic interconnects, to be used in Intermediate Temperature Solid Oxide Fuel Cells. (C) 2004 Elsevier B.V. All rights reserved.
引用
收藏
页码:98 / 103
页数:6
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