Combined application of analytical techniques for the characterization of polymer supported species

被引：19

作者：

Grice, P ^{[1
]}

Leach, AG ^{[1
]}

Ley, SV ^{[1
]}

Massi, A ^{[1
]}

Mynett, DM ^{[1
]}

机构：

[1] Univ Cambridge, Dept Chem, Cambridge CB2 1EW, England

来源：

JOURNAL OF COMBINATORIAL CHEMISTRY | 2000年 / 2卷 / 05期

关键词：

D O I：

10.1021/cc000021p

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

The combined application of a diverse range of analytical techniques is described for the complete analysis of polymer supported molecules. These techniques permit complete description of the FTIR, H-1 NMR, and C-13. NMR spectra. The comparison of supported bicyclo[2.2.2]octane derivatives with analogous species prepared using polymer supported reagents is made.

引用

页码：491 / 495

页数：5

共 49 条

[1] ANALYTICAL TECHNIQUES IN COMBINATORIAL CHEMISTRY - MAS CH CORRELATION IN SOLVENT-SWOLLEN RESIN
ANDERSON, RC
JAREMA, MA
SHAPIRO, MJ
STOKES, JP
ZILIOX, M
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1995, 60 (09) : 2650 - 2651
[2] STRUCTURE DETERMINATION IN COMBINATORIAL CHEMISTRY - UTILIZATION OF MAGIC-ANGLE-SPINNING HMQC AND TOCSY NMR-SPECTRA IN THE STRUCTURE DETERMINATION OF WANG-BOUND LYSINE
ANDERSON, RC
STOKES, JP
SHAPIRO, MJ
[J]. TETRAHEDRON LETTERS, 1995, 36 (30) : 5311 - 5314
[3] POLYMERS FOR CATALYTIC CATION RADICAL CHEMISTRY
BAULD, NL
BELLVILLE, DJ
GARDNER, SA
MIGRON, Y
COGSWELL, G
[J]. TETRAHEDRON LETTERS, 1982, 23 (08) : 825 - 828
[4] Development of a polymer bound Wittig reaction and use in multi-step organic synthesis for the overall conversion of alcohols to β-hydroxyamines
Bolli, MH
Ley, SV
[J]. JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1998, (15): : 2243 - 2246
[5] Synthesis of an array of potential matrix metalloproteinase inhibitors using a sequence of polymer-supported reagents
Caldarelli, M
Habermann, J
Ley, SV
[J]. BIOORGANIC & MEDICINAL CHEMISTRY LETTERS, 1999, 9 (14) : 2049 - 2052
[6] Clean five-step synthesis of an array of 1,2,3,4-tetra-substituted pyrroles using polymer-supported reagents
Caldarelli, M
Habermann, J
Ley, SV
[J]. JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1999, (02): : 107 - 110
[7] High throughput on-bead monitoring of solid phase reactions by diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS)
Chan, TY
Chen, R
Sofia, MJ
Smith, BC
Glennon, D
[J]. TETRAHEDRON LETTERS, 1997, 38 (16) : 2821 - 2824
[8] 2D SECSY NMR for combinatorial chemistry. High-resolution MAS spectra for resin-bound molecules
Chin, J
Fell, B
Pochapsky, S
Shapiro, MJ
Wareing, JR
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1998, 63 (04) : 1309 - 1311
[9] Dewry D.H., 1999, MED RES REV, V19, P97
[10] Magic angle spinning nuclear magnetic resonance in solid-phase peptide synthesis
Dhalluin, C
Boutillon, C
Tartar, A
Lippens, G
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1997, 119 (43) : 10494 - 10500

← 1 2 3 4 5 →