Temperature distribution of wedge-shaped specimen in TEM

被引:7
作者
Chen, Lu
Wang, Yong [1 ]
Zhang, Ze [1 ]
机构
[1] Zhejiang Univ, Sch Mat Sci & Engn, Ctr Electron Microscopy, Hangzhou 310027, Zhejiang, Peoples R China
基金
中国国家自然科学基金;
关键词
Electron irradiation; Heating effect; FIB specimen; In-situ TEM; FOCUSED ION-BEAM; ELECTRON; DAMAGE;
D O I
10.1016/j.micron.2018.04.007
中图分类号
TH742 [显微镜];
学科分类号
080401 [精密仪器及机械];
摘要
Understanding the electron irradiation effects, especially the heating effect, is very important to the in-situ TEM experiments. A model is established to describe the temperature distribution of FIB prepared wedge-shaped specimen induced by electron irradiation, and a Cu2Se specimen is presented to estimate the temperature distribution inside the observed area under different dose rates in an in-situ TEM heating experiments. The result indicates that in normal situations, the electron irradiation caused temperature inhomogeneity inside the observed area is ignorable.
引用
收藏
页码:46 / 49
页数:4
相关论文
共 15 条
[1]
Chen L., UNPUB
[2]
BEAM HEATING IN AN ASYMMETRICALLY ILLUMINATED THIN CIRCULAR FILM [J].
CURZON, AE .
JOURNAL OF MICROSCOPY-OXFORD, 1992, 167 :303-311
[3]
In situ observation of heat-induced degradation of perovskite solar cells [J].
Divitini, G. ;
Cacovich, S. ;
Matteocci, F. ;
Cina, L. ;
Di Carlo, A. ;
Ducati, C. .
NATURE ENERGY, 2016, 1
[4]
Convenient Preparation of High-Quality Specimens for Annealing Experiments in the Transmission Electron Microscope [J].
Duchamp, Martial ;
Xu, Qiang ;
Dunin-Borkowski, Rafal E. .
MICROSCOPY AND MICROANALYSIS, 2014, 20 (06) :1638-1645
[5]
Radiation damage in the TEM and SEM [J].
Egerton, RF ;
Li, P ;
Malac, M .
MICRON, 2004, 35 (06) :399-409
[6]
Garslaw HS., 1959, Conduction of Heat in Solids, V2nd ed
[7]
Ishitani T, 1996, MICROSC RES TECHNIQ, V35, P320, DOI 10.1002/(SICI)1097-0029(19961101)35:4<320::AID-JEMT3>3.0.CO
[8]
2-Q
[9]
QUANTITATIVE-ANALYSIS OF KNOCK-ON AND THERMAL-DAMAGE OF BIOLOGICAL SPECIMENS BY ELECTRON-IRRADIATION IN TRANSMISSION ELECTRON-MICROSCOPY [J].
KANAYA, K ;
ADACHI, K ;
YONEHARA, K ;
MURANAKA, Y ;
ISHIKAWA, H .
MICRON AND MICROSCOPICA ACTA, 1991, 22 (03) :223-237
[10]
Three-dimensional nanofabrication of polystyrene by focused ion beam [J].
Lee, C. C. ;
Proust, G. ;
Alici, G. ;
Spinks, G. M. ;
Cairney, J. M. .
JOURNAL OF MICROSCOPY, 2012, 248 (02) :129-139