Photocrystallography - design and methodology for the use of a light-emitting diode device

被引：32

作者：

Brayshaw, Simon K. ^{[1
]}

Knight, Jason W. ^{[2
]}

Raithby, Paul R. ^{[1
]}

Savarese, Teresa L. ^{[1
]}

Schiffers, Stefanie ^{[1
]}

Teat, Simon J. ^{[2
]}

Warren, John E. ^{[1
,3
]}

Warren, Mark R. ^{[1
]}

机构：

[1] Univ Bath, Dept Chem, Bath BA2 7AY, Avon, England

[2] Univ Calif Berkeley, Lawrence Berkeley Lab, Adv Light Source, Berkeley, CA 94721 USA

[3] STFC Daresbury Lab, Warrington WA4 4AD, Cheshire, England

来源：

JOURNAL OF APPLIED CRYSTALLOGRAPHY | 2010年 / 43卷

基金：

英国工程与自然科学研究理事会;

关键词：

X-RAY-DIFFRACTION; SUPRAMOLECULAR SOLIDS; SINGLE-CRYSTAL; EXCITED-STATE; CRYSTALLOGRAPHY; EXCITATION; COMPLEXES; ISOMER;

D O I：

10.1107/S0021889810004759

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

With the increase in interest in photocrystallographic experiments, the use of light-emitting diodes (LEDs) provides an alternative, low-budget light source (by comparison to lasers) and allows photocrystallographic experiments to be carried out readily. Here the design of an LED array device suitable for use in single-crystal X-ray diffraction experiments is reported, and the experimental methodology used for determining the structures of metastable species is described.

引用

页码：337 / 340

页数：4

共 24 条

[1] Photocrystallographic structure determination of a new geometric isomer of [Ru(NH3)4(H2O)(η1-OSO)][MeC6H4SO3]2 [J].