SPATIAL-RESOLUTION IN SELECTED-AREA EELS

被引:10
作者
SCHENNER, M
SCHATTSCHNEIDER, P
机构
[1] Institut für Angewandte und Technische Physik, Technische Universität Wien, A-1040 Wien
关键词
D O I
10.1016/0304-3991(94)90078-7
中图分类号
TH742 [显微镜];
学科分类号
摘要
We investigate the effect of objective-lens chromatic aberration on quantitative chemical microanalysis using electron energy-loss spectrometry in the electron microscope. Experimental tests were done on a specimen with a planar interface under the condition of a rather large chromatic error in image mode. We discuss three different models of image formation with inelastically scattered electrons. Simulations for Ni show that the quantum-mechanical image theory for large defocus values is practically equivalent to a Lorentzian image distribution and describes the experimental data satisfactorily. A method to obtain a proper defocus setting for the compensation of the chromatic error is also presented.
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收藏
页码:31 / 41
页数:11
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