CAPILLARY GAS-CHROMATOGRAPHY OF SOME TRIGLYCERIDES IN CHEESE USING PROGRAMMED-TEMPERATURE INJECTION

被引：13

作者：

ALONSO, L

机构：

[1] Instituto de Productos Lácteos de Asturias (CSIC), Villaviciosa, Austrias, 33300, Carretera de Infiesto

来源：

CHROMATOGRAPHIA | 1993年 / 35卷 / 9-12期

关键词：

GAS CHROMATOGRAPHY; TRIGLYCERIDES IN CHEESE; PROGRAM TEMPERATURE (PTV) INJECTION; SILICA CAPILLARY COLUMNS;

D O I：

10.1007/BF02267931

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A rapid gas chromatographic method for the analysis of triglycerides in cheese on a capillary column with a programmed temperature vaporizer has been developed. Fat were extracted with hexane to dryness. The reproducibility of the method was assessed and the coefficient of variation for the total triglycerides was 2.50 %. Recovery of individual triglycerides ranged between 87 to 105 %.

引用

页码：649 / 652

页数：4

共 16 条

[1] BARRON LJR, 1992, J DAIRY RES, V57, P517
[2] ANALYSIS OF MILKFAT BY HPLC
FREDE, E
THIELE, H
[J]. JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1987, 64 (04) : 521 - 528
[3] CAPILLARY GC OF TRIGLYCERIDES IN FATS AND OILS USING A HIGH-TEMPERATURE PHENYLMETHYLSILICONE STATIONARY PHASE .2. THE ANALYSIS OF CHOCOLATE FATS
GEERAERT, E
SANDRA, P
[J]. JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1987, 64 (01) : 100 - 105
[4] HINRICHS J, 1992, MILCHWISSENSCHAFT, V47, P495
[5] ANALYSIS OF TRIGLYCERIDES BY CAPILLARY GAS-CHROMATOGRAPHY WITH PROGRAMMED-TEMPERATURE INJECTION
HINSHAW, JV
SEFEROVIC, W
[J]. JOURNAL OF HIGH RESOLUTION CHROMATOGRAPHY & CHROMATOGRAPHY COMMUNICATIONS, 1986, 9 (12): : 731 - 736
[6] JUAREZ M, 1983, REV AGROQUIM TECNOL, V23, P467
[7] IMPROVED GAS-CHROMATOGRAPHIC METHOD FOR THE DETERMINATION OF THE INDIVIDUAL FREE FATTY-ACIDS IN CHEESE USING A CAPILLARY COLUMN AND A PTV INJECTOR
JUAREZ, M
DELAFUENTE, MA
FONTECHA, J
[J]. CHROMATOGRAPHIA, 1992, 33 (7-8) : 351 - 355
[8] JUAREZ M, 1980, ALIMENTARIA, V109, P61
[9] TRIGLYCERIDE STRUCTURE OF MILK FATS
KUKSIS, A
MARAI, L
MYHER, JJ
[J]. JOURNAL OF THE AMERICAN OIL CHEMISTS SOCIETY, 1973, 50 (06) : 193 - 201
[10] LUND P, 1988, MILCHWISSENSCHAFT, V43, P159

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