RAPID REDUCTION OF SULFONES TO SULFIDES USING LIALH4-TICL4

被引：24

作者：

AKGUN, E

MAHMOOD, K

MATHIS, CA

机构：

[1] UNIV PITTSBURGH,DEPT RADIOL,PITTSBURGH,PA 15213

[2] UNIV PITTSBURGH,DEPT PHARMACEUT SCI,PITTSBURGH,PA 15213

来源：

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS | 1994年 / 06期

关键词：

D O I：

10.1039/c39940000761

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A variety of sulfones are reduced rapidly to sulfides in high yields using lithium aluminium hydride-titanium tetrachloride in tetrahydrofuran.

引用

页码：761 / 762

页数：2

共 19 条

[1] THE REDUCTION OF SULFONES TO SULFIDES [J].

BORDWELL, FG ;

MCKELLIN, WH .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1951, 73 (05) :2251-2253

[2]

DRABOWICZ J, 1976, SYNTHESIS-STUTTGART, P527

[3] REDUCTION OF SULFOXIDES - A REVIEW [J].

DRABOWICZ, J ;

TOGO, H ;

MIKOLAJCZYK, M ;

OAE, S .

ORGANIC PREPARATIONS AND PROCEDURES INTERNATIONAL, 1984, 16 (3-4) :171-198

[4] FACILE REDUCTION OF SULFONES TO SULFIDES [J].

GARDNER, JN ;

KAISER, S ;

KRUBINER, A ;

LUCAS, H .

CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE, 1973, 51 (09) :1419-1421

[5] RAPID AND MILD DEOXYGENATION OF ORGANOHETEROATOM OXIDES WITH THE EFFICIENT ELECTRON-TRANSFER SYSTEM SMI2 TETRAHYDROFURAN HEXAMETHYLPHOSPHORIC TRIAMIDE [J].

HANDA, Y ;

INANAGA, J ;

YAMAGUCHI, M .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1989, (05) :298-299

[6] ADDITIVE AND SOLVENT EFFECTS ON SMI2 REDUCTIONS - THE EFFECTS OF WATER AND DMPU [J].

HASEGAWA, E ;

CURRAN, DP .

JOURNAL OF ORGANIC CHEMISTRY, 1993, 58 (18) :5008-5010

[7] THE NOVEL REDUCTION OF PYRIDINE-DERIVATIVES WITH SAMARIUM DIIODIDE [J].

KAMOCHI, Y ;

KUDO, T .

HETEROCYCLES, 1993, 36 (10) :2383-2396

[8]

KANO S, 1980, SYNTHESIS-STUTTGART, P695

[9] REDUCTIVE DESULFONYLATION OF PHENYL SULFONES BY SAMARIUM(II) IODIDE-HEXAMETHYLPHOSPHORIC TRIAMIDE [J].

KUNZER, H ;

STAHNKE, M ;

SAUER, G ;

WIECHERT, R .

TETRAHEDRON LETTERS, 1991, 32 (17) :1949-1952

[10] RECENT DEVELOPMENTS IN SULFONE CHEMISTRY [J].

MAGNUS, PD .

TETRAHEDRON, 1977, 33 (16) :2019-2045

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