陈皮中川陈皮素的提取分离及改性

被引：16

作者：

罗世坤 ^{[1
]}

王家欢 ^{[1
]}

徐兰英 ^{[1
]}

龙涛 ^{[1
]}

李士明 ^{[1
,2
]}

机构：

[1] 黄冈师范学院化工学院,催化材料制备及应用湖北省重点实验室

[2] 罗格斯大学食品科学系

来源：

食品科学 | 2014年 / 35卷 / 24期

关键词：

陈皮; 分离纯化; 多甲氧基黄酮; 川陈皮素; 5-去甲基川陈皮素;

D O I：

暂无

中图分类号：

TS209 [食品工业副产品加工与利用];

学科分类号：

083203 [农产品加工及贮藏工程];

摘要：

以陈皮中川陈皮素的提取、分离纯化以及改性为目的,采用无水乙醇浸提陈皮得浸膏,以氯仿为萃取剂萃取浸膏,得到多甲氧基黄酮混合物,再以硅胶为吸附剂、乙酸乙酯和石油醚的混合液为洗脱剂,采用柱色谱法分离多甲氧基黄酮化合物,经高效液相色谱和气相色谱-质谱检测并与标准品对比,最终确证得到川陈皮素纯品。研究从川陈皮素到5-去甲基川陈皮素的合成路线,优化了改性条件,在浓盐酸与无水乙醇体积比为1∶9条件下,将川陈皮素加热回流反应24 h,可以得到纯度大于97%的5-去甲基川陈皮素。

引用

页码：20 / 23

页数：4

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