Off-line SFE-CZE analysis of carbamates residues in tobacco samples

被引：20

作者：

Lancas, FM

Rissato, SR

Galhiane, MS

机构：

[1] University of São Paulo, Institute of Chemistry of So Carlos, São Carlos (SP), 13560-970

来源：

CHROMATOGRAPHIA | 1996年 / 42卷 / 5-6期

关键词：

supercritical fluid extraction; capillary electrophoresis; carbamates residues; tobacco samples;

D O I：

10.1007/BF02290318

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Determination of carbamate residues in tobacco samples was carried out by solid-liquid extraction (SLE) and supercritical-fluid extraction (SFE) methods, both developed for this purpose. The clean-up step was carried out on SPE-Florisil cartridges and the extracts analysed by capillary zone electrophoresis (CZE) with UV detection. The results were compared and SFE using CO2-acetone showed the best results in terms of recovery and generally higher extraction power. SFE in conjunction with CZE proved suitable for carbamate residue analysis in real tobacco samples.

引用

页码：323 / 328

页数：6

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