Microwave-solvothermal synthesis of nanocrystalline cadmium sulfide

被引：124

作者：

Murugan, AV ^{[1
]}

Sonawane, RS ^{[1
]}

Kale, BB ^{[1
]}

Apte, SK ^{[1
]}

Kulkarni, AV ^{[1
]}

机构：

[1] Govt India, Minist Informat Technol, Ctr Mat Elect Technol, Pune 411008, Maharashtra, India

来源：

MATERIALS CHEMISTRY AND PHYSICS | 2001年 / 71卷 / 01期

关键词：

microwave-solvothermal synthesis; cadmium sulfide; hexagonal;

D O I：

10.1016/S0254-0584(00)00533-2

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

The microwave assisted synthesis is generally much faster, cleaner and more economical than the conventional methods. The combination of microwave and hydrothermal techniques has been used Ill the last few years for the synthesis of nanocrystalline powders. We present here a versatile process of novel microwave-solvothermal technique for synthesizing nanocrystalline CdS particles. The effect of different parameters such as time, temperature, solvents and molar ratio of Cd2+ to thiourea on the phase(s) formation of nanocrystalline cadmium sulfide under micrawave-solvothermal conditions using microwaves of 2.45 GHz frequency are investigated. The obtained CdS is characterized by the powder X-ray diffraction and SEM. (C) 2001 Elsevier Science B.V. All rights reserved.

引用

页码：98 / 102

页数：5

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