Helping to authenticate sparkling drinks with 13C/12C of CO2 by gas chromatography-isotope ratio mass spectrometry

被引:31
作者
Calderone, Giovanni
Guillou, Claude
Reniero, Fabiano
Naulet, Norbert
机构
[1] Commiss European Communities, Joint Res Ctr, Inst Hlth & Consumer Protect, Phys & Chem Exposure Unit, I-20127 Milan, VA, Italy
[2] CNRS, LAIEM, F-44322 Nantes 3, France
关键词
food authentication; stable isotope ratio methods in food; carbon dioxide; ethanol; delta C-13; GC-C-IRMS; IRMS; sparkling wine; beer; carbonated water; carbonated drinks; multi isotopic analysis; H-2-SNIF-NMR;
D O I
10.1016/j.foodres.2006.10.001
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
We applied direct injections of headspace gas into a Gas Chromatography - Combustion - Isotope Ratio Mass Spectrometry (GC-C-IRMS) system to measure C-13/C-12 isotopic ratio of carbon dioxide from the headspace of several sparkling and soft-drinks. This straightforward technique, which consists in an automated analysis of the headspace sample with no prior purification steps, improves the determination of delta C-13 values of CO2 gas as a food probe authenticity. However, for an ultimate test, combination with other isotopic data is required. (c) 2006 Elsevier Ltd. All rights reserved.
引用
收藏
页码:324 / 331
页数:8
相关论文
共 25 条
[11]   NATURAL FACTORS OF SITE-SPECIFIC ISOTOPE FRACTIONATION OF HYDROGEN IN THE FERMENTATION PRODUCTS (ETHANOL AND WATER) OF BARLEY [J].
FRANCONI, JM ;
NAULET, N ;
MARTIN, GJ .
JOURNAL OF CEREAL SCIENCE, 1989, 10 (01) :69-80
[12]   Contribution to the study of the origin of CO2 in Spanish sparkling wines by determination of the C-13/C-12 isotope ratio [J].
GonzalezMartin, I ;
GonzalezPerez, C ;
MarquesMacias, E .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1997, 45 (04) :1149-1151
[13]   ONLINE PURIFICATION AND C-13 ISOTOPIC ANALYSIS OF CARBON-DIOXIDE IN BREATH - EVALUATION OF ONLINE GAS-CHROMATOGRAPHY ISOTOPE RATIO MASS-SPECTROMETRY [J].
GUILLUY, R ;
BILLIONREY, F ;
PACHIAUDI, C ;
NORMAND, S ;
RIOU, JP ;
JUMEAU, EJ ;
BRAZIER, JL .
ANALYTICA CHIMICA ACTA, 1992, 259 (02) :193-202
[14]   PHOTOSYNTHETIC CO2-FIXATION PATHWAYS [J].
HATCH, MD ;
SLACK, CR .
ANNUAL REVIEW OF PLANT PHYSIOLOGY, 1970, 21 :141-+
[15]   REVERSE ISOTOPE-DILUTION ANALYSIS OF (CO2)-C-13 USING GAS-CHROMATOGRAPHY ISOTOPE RATIO MASS-SPECTROMETRY - APPLICATION TO THE QUANTITATIVE-DETERMINATION OF (CO2)-C-13, RELEASED BY HUMAN POLYMORPHONUCLEAR LEUKOCYTES [J].
LAMRINI, R ;
LACAN, P ;
FRANCINA, A ;
GUILLUY, R ;
BRAZIER, JL .
RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 1995, 9 (11) :1017-1020
[16]   APPLICATION OF SITE-SPECIFIC NATURAL ISOTOPE FRACTIONATION (SNIF-NMR) OF HYDROGEN TO THE CHARACTERIZATION OF EUROPEAN BEERS [J].
MARTIN, GJ ;
BENBERNOU, M ;
LANTIER, F .
JOURNAL OF THE INSTITUTE OF BREWING, 1985, 91 (04) :242-249
[17]   Stable carbon isotopic composition of the wine and CO2 bubbles of sparkling wines:: Detecting C4 sugar additions [J].
Martinelli, LA ;
Moreira, MZ ;
Ometto, JPHB ;
Alcarde, AR ;
Rizzon, LA ;
Stange, E ;
Ehleringer, JR .
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2003, 51 (09) :2625-2631
[18]   Applied gas chromatography coupled to isotope ratio mass spectrometry [J].
Meier-Augenstein, W .
JOURNAL OF CHROMATOGRAPHY A, 1999, 842 (1-2) :351-371
[19]   Origin, transport and discharge of CO2 in central Italy [J].
Minissale, A .
EARTH-SCIENCE REVIEWS, 2004, 66 (1-2) :89-141
[20]   A rapid and precise technique for measuring δ13C-CO2 and δ18O-CO2 ratios at ambient CO2 concentrations for biological applications and the influence of container type and storage time on the sample isotope ratios [J].
Mortazavi, B ;
Chanton, JP .
RAPID COMMUNICATIONS IN MASS SPECTROMETRY, 2002, 16 (14) :1398-1403