Synthesis and characterization of ZnO, CuO and a mixed Zn and Cu oxide

被引：186

作者：

Fernandes, D. M. ^{[1
]}

Silva, R. ^{[1
]}

Hechenleitner, A. A. Winkler ^{[1
]}

Radovanovic, E. ^{[1
]}

Melo, M. A. Custodio ^{[2
]}

Pineda, E. A. Gomez ^{[1
]}

机构：

[1] Univ Estadual Maringa, Dept Quim, BR-87020900 Maringa, Parana, Brazil

[2] Univ Estadual Maringa, Dept Fis, BR-87020900 Maringa, Parana, Brazil

来源：

MATERIALS CHEMISTRY AND PHYSICS | 2009年 / 115卷 / 01期

关键词：

Nanostructures; Ceramics; X-ray diffraction; Scanning electron microscopy; LOW-TEMPERATURE SYNTHESIS; OPTICAL-PROPERTIES; ZINC-OXIDE; NANOPARTICLES; POWDERS;

D O I：

10.1016/j.matchemphys.2008.11.038

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

ZnO, CuO, and Cu0.05Zn0.95O nanoparticles have been prepared by a sol-gel method using poly(vinyl alcohol) aqueous solutions and metal nitrate precursors. The precursor powders were analyzed by thermogravimetry (TG) and differential scanning calorimetry (DSC). X-ray powder diffractometry (XRD), infrared spectroscopy (FTIR), and scanning electron microscopy (SEM) were used to characterize the structural and the chemical features of the nanoparticles. An average nanocrystallite size of 25-30 nm was obtained for ZnO and Cu0.05Zn0.95O and of 40 nm for CuO, as estimated by the Scherrer's equation. (C) 2008 Elsevier B.V. All rights reserved.

引用

页码：110 / 115

页数：6

共 33 条

[11] A convenient alcohothermal approach for low temperature synthesis of CuO nanoparticles [J].

Hong, ZS ;

Cao, Y ;

Deng, JF .

MATERIALS LETTERS, 2002, 52 (1-2) :34-38

[12] Preparation of Co3O4 nanoparticles by a polymer combustion route [J].

Jiu, JT ;

Ge, Y ;

Li, XN ;

Nie, L .

MATERIALS LETTERS, 2002, 54 (04) :260-263

[13] Synthesis of nanocrystalline zirconia powders for TZP ceramics by a nitrate-citrate combustion route [J].

Juárez, RE ;

Lamas, DG ;

Lascalea, GE ;

de Reca, NEW .

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2000, 20 (02) :133-138

[14] Planar defect of the nano-structured zinc oxide as the site for stabilization of the copper active species in Cu/ZnO catalysts [J].

Khassin, AA ;

Pelipenko, VV ;

Minyukova, TP ;

Zaikovskii, VI ;

Kochubey, DI ;

Yurieva, TM .

CATALYSIS TODAY, 2006, 112 (1-4) :143-147

[15]

Klingshirm C.F., 1995, SEMICONDUCTOR OPTICS, P309

[16] Modification in optical properties of negative Cu ion implanted ZnO [J].

Kono, K ;

Arora, SK ;

Kishimoto, N .

NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 2003, 206 :291-294

[17] Nanostructure and chemical state of nanocomposites prepared by Co-sputtering method [J].

Koshizaki, N ;

Yasumoto, K ;

Terauchi, S ;

Umehara, H ;

Sasaki, T ;

Oyama, T .

NANOSTRUCTURED MATERIALS, 1997, 9 (1-8) :587-590

[18] Sonochemical synthesis and characterization of nanometer-size transition metal oxides from metal acetates [J].

Kumar, RV ;

Diamant, Y ;

Gedanken, A .

CHEMISTRY OF MATERIALS, 2000, 12 (08) :2301-2305

[19] Synthesis and characterization of nanocrystalline powders for partially stabilized zirconia ceramics [J].

Lamas, DG ;

Lascalea, GE ;

de Reca, NEW .

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 1998, 18 (09) :1217-1221

[20] Catalyst-free growth of ZnO nanowires by metal-organic chemical vapour deposition (MOCVD) and thermal evaporation [J].

Lee, W ;

Jeong, MC ;

Myoung, JM .

ACTA MATERIALIA, 2004, 52 (13) :3949-3957

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