Bonded cellulose-derived high-performance liquid chromatography chiral stationary phases -: III.: Effect of the reticulation of the cellulose derivative on performance

被引：33

作者：

Franco, P

Minguillón, C

Oliveros, L

机构：

[1] Univ Barcelona, Fac Farm, Quim Farmaceut Lab, E-08028 Barcelona, Spain

[2] Conservatoire Natl Arts & Metiers, Lab Chim Gen, F-75141 Paris 03, France

来源：

JOURNAL OF CHROMATOGRAPHY A | 1997年 / 791卷 / 1-2期

关键词：

chiral stationary phases; LC; enantiomer separation; cellulose stationary phases; lorazepam; warfarin; naproxen; beta-blockers;

D O I：

10.1016/S0021-9673(97)00836-4

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The influence of the reticulation of a mixed 10-undecenoyl/3,5-dimethylphenylaminocarbonyl derivative of cellulose on the enantioselectivity of several high-performance liquid chromatography (HPLC) chiral stationary phases (CSPs) was investigated. Three cellulose-derived chiral columns were obtained by reticulation of the same cellulose derivative on three end-capped silica gels of different pore size. The performance of the obtained supports was studied and compared with that of three bonded cellulose-derived CSPs prepared by fixation of the same cellulose derivative on allylsilica gel. (C) 1997 Elsevier Science B.V.

引用

页码：37 / 44

页数：8

共 15 条

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