Synthesis of colloidal magnetite nanocrystals using high molecular weight solvent

被引：45

作者：

Goncalves, Ricardo H. ^{[1
]}

Cardoso, Claudio A. ^{[2
]}

Leite, Edson R. ^{[1
]}

机构：

[1] Univ Fed Sao Carlos, Dept Chem, BR-13565905 Sao Carlos, SP, Brazil

[2] Univ Fed Sao Carlos, Dept Phys, BR-13565905 Sao Carlos, SP, Brazil

来源：

JOURNAL OF MATERIALS CHEMISTRY | 2010年 / 20卷 / 06期

基金：

巴西圣保罗研究基金会;

关键词：

IRON-OXIDE NANOPARTICLES; DRUG-DELIVERY; SURFACE MODIFICATION; POLYMERIC MICELLES; QUANTUM DOTS; SIZE; FUNCTIONALIZATION; MICROSPHERES; RESONANCE; FLUIDS;

D O I：

10.1039/b917030h

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

In this work, we describe a single-step synthetic route to obtain magnetic nanocrystals (MN), Fe3O4 nanocrystals, soluble in different solvents. To synthesize grafted MN in a single step, we used a high molecular weight solvent (a polyol) that can be attached to the particle surface, which then transfers its solubility to the particle. Using polyols with different molecular weights and polarity enabled us to control the size, aggregation and morphology. The solubility behavior of the MN confirms our success in transferring the solubility of the adsorbed polymer to the nanocrystal.

引用

页码：1167 / 1172

页数：6

共 39 条

[11] Environmentally-friendly preparation of water-dispersible magnetite nanoparticles [J].

Jia, Xiao ;

Chen, Dairong ;

Jiao, Xiuling ;

Zhai, Shumei .

CHEMICAL COMMUNICATIONS, 2009, (08) :968-970

[12] Multifunctional Uniform Nanoparticles Composed of a Magnetite Nanocrystal Core and a Mesoporous Silica Shell for Magnetic Resonance and Fluorescence Imaging and for Drug Delivery [J].

Kim, Jaeyun ;

Kim, Hoe Suk ;

Lee, Nohyun ;

Kim, Taeho ;

Kim, Hyoungsu ;

Yu, Taekyung ;

Song, In Chan ;

Moon, Woo Kyung ;

Hyeon, Taeghwan .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2008, 47 (44) :8438-8441

[13] Incorporation of Fe3O4 Nanoparticles into Organometallic Coordination Polymers by Nanoparticle Surface Modification [J].

Kim, Sang Bok ;

Cai, Chen ;

Sun, Shoutheng ;

Sweigart, Dwight A. .

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2009, 48 (16) :2907-2910

[14] Controlling transport and chemical functionality of magnetic nanoparticles [J].

Latham, Andrew H. ;

Williams, Mary Elizabeth .

ACCOUNTS OF CHEMICAL RESEARCH, 2008, 41 (03) :411-420

[15] Synthesis of amphiphilic superparamagnetic ferrite/block copolymer hollow submicrospheres [J].

Li, Xin-Hao ;

Zhang, Dong-Hui ;

Chen, Jie-Sheng .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2006, 128 (26) :8382-8383

[16] One-pot reaction to synthesize biocompatible magnetite nanoparticles [J].

Li, Z ;

Wei, L ;

Gao, MY ;

Lei, H .

ADVANCED MATERIALS, 2005, 17 (08) :1001-+

[17] Design of an amphiphilic polymer for nanoparticle coating and functionalization [J].

Lin, Cheng-An J. ;

Sperling, Ralph A. ;

Li, Jimmy K. ;

Yang, Ting-Ya ;

Li, Pei-Yun ;

Zanella, Marco ;

Chang, Walter H. ;

Parak, Wolfgang J. .

SMALL, 2008, 4 (03) :334-341

[18] Modifying the surface properties of superparamagnetic iron oxide nanoparticles through a sol-gel approach [J].

Lu, Y ;

Yin, YD ;

Mayers, BT ;

Xia, YN .

NANO LETTERS, 2002, 2 (03) :183-186

[19] PREPARATION OF AQUEOUS MAGNETIC LIQUIDS IN ALKALINE AND ACIDIC MEDIA [J].

MASSART, R .

IEEE TRANSACTIONS ON MAGNETICS, 1981, 17 (02) :1247-1248

[20] Targeted delivery of multifunctional magnetic nanoparticles [J].

McCarthy, Jason R. ;

Kelly, Kimberly A. ;

Sun, Eric Y. ;

Weissleder, Ralph .

NANOMEDICINE, 2007, 2 (02) :153-167

← 1 2 3 4 →