Accurate structure determination from image reconstruction in ADF STEM

被引:86
作者
Nellist, PD
Pennycook, SJ
机构
[1] Univ Cambridge, Cavendish Lab, Cambridge CB3 0HE, England
[2] Oak Ridge Natl Lab, Div Solid State, Oak Ridge, TN 37831 USA
来源
JOURNAL OF MICROSCOPY-OXFORD | 1998年 / 190卷
关键词
ADF; image reconstruction; incoherent imaging; probe reconstruction; STEM; structure determination;
D O I
10.1046/j.1365-2818.1998.3260881.x
中图分类号
TH742 [显微镜];
学科分类号
摘要
Annular dark-field (ADF) imaging in a scanning transmission electron microscope results in direct structure images of the atomic configuration of the specimen. Since such images are almost perfectly incoherent they can be treated as a convolution between a point-spread function, which is simply the intensity of the illuminating electron probe, and a sharply peaked object function that represents the projected structure of the specimen. Knowledge of the object function for an image region of perfect crystal allows the point-spread function to be directly determined for that image. We examine how the object function for an image can then be reconstructed using a Wiener filter, the CLEAN algorithm and a maximum entropy reconstruction, Prior information is required to perform a reconstruction, and we discuss what nature of prior information is suitable for ADF imaging.
引用
收藏
页码:159 / 170
页数:12
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