共 30 条
Synthesis, characterisation and adsorption properties of microporous scandium carboxylates with rigid and flexible frameworks
被引:170
作者:

Mowat, John P. S.
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Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland

Miller, Stuart R.
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Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland
Univ Versailles St Quentin Yvelines, Inst Lavoisier, F-78035 Versailles, France Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland

Slawin, Alexandra M. Z.
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Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland

Seymour, Valerie R.
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Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland

Ashbrook, Sharon E.
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Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland

Wright, Paul A.
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Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland
机构:
[1] Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland
[2] Univ Versailles St Quentin Yvelines, Inst Lavoisier, F-78035 Versailles, France
基金:
英国工程与自然科学研究理事会;
关键词:
Scandium carboxylates;
Microporous MOFs;
MIL-53;
CO2;
adsorption;
Sc-45 MAS NMR;
METAL-ORGANIC-FRAMEWORKS;
BUILDING-BLOCKS;
CARBON-DIOXIDE;
TEREPHTHALATE;
MIL-53;
TOPOLOGY;
SOLIDS;
BENZENEDICARBOXYLATE;
SC-2(O2CC6H4CO2)(3);
DIFFRACTION;
D O I:
10.1016/j.micromeso.2010.12.016
中图分类号:
O69 [应用化学];
学科分类号:
081704 ;
摘要:
Conditions for the synthesis of each of the scandium terephthalate frameworks Sc2L3, MIL-53(Sc) (Sc(OH)L) and MIL-88(Sc) (Sc3O(H2O)(2)(OH)L-3) (L = 1.4-benzenedicarboxylate (BDC)) have been established. In addition, the MOFs MIL-100(Sc) (Sc3O(H2O)(2)(OH)L'(2), L' = 1,3,5-benzenetricarboxylate (BTC)) and socMOF (Sc3O(H2O)(3),(NO3-)L ''(1.5), L '' = 3,3',5,5'-azobenzenetetracarboxylate (ABTC)), have been synthesised for the first time with Sc. These materials have been characterised by powder and single crystal X-ray diffraction, H-1, C-13 and Sc-45 MAS NMR, and gas adsorption. MIL-53(Sc) is a highly flexible breathing framework that adopts many different forms, depending on the amount and type of adsorbate included. The structures of the as-prepared solvent-containing form, MIL-53(Sc)-DMF (DMF = dimethylformamide) and of the desolvated, hydrated form, MIL-53(Sc)-H2O, have been determined. The former structure possesses one kind of partially open channel, whereas the latter includes two kinds of channel, closed and slightly open. The hydrated structure's configuration has not previously been observed for MIL-53 materials. 45Sc MAS NMR is a sensitive probe for the Sc environment: distinctive lineshapes are observed for isolated ScO6 octahedra, corner-sharing chains of ScO4(OH)(2) octahedra and Sc3O(O2C-)(6)(OH, H2O)(3) trimers of octahedra. N-2 adsorption at 77 K indicates that the flexible frameworks MIL-88(Sc) and MIL-53(Sc) show no porosity in their desolvated, closed forms, whilst the rigid frameworks Sc2BDC3 (0.26 cm(3) g(-1)), MIL-100(Sc) (0.72 cm(3) g(-1)) and Sc-ABTC (0.57 cm(3) g(-1)) have so far been prepared with appreciable permanent porosity. For CO2 adsorption on desolvated solids, remarkable behaviour is shown by the flexible MIL-53(Sc), which opens in two stages to a maximum capacity of >13 mmol g(-1), while the rigid frameworks show uptakes at 196 K (at p/p(o) = 0.40) of 5.5 mmol g(-1) (Sc2BDC3), 21.3 mmol g(-1) (MIL-100(Sc)) and 13.1 mmol g(-1) (Sc-ABTC). (C) 2010 Elsevier Inc. All rights reserved.
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页码:322 / 333
页数:12
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Univ S Florida, Dept Chem, Tampa, FL 33620 USA Inst Nichtklass Chem eV, D-04318 Leipzig, Germany

Cairns, A. J.
论文数: 0 引用数: 0
h-index: 0
机构:
Univ S Florida, Dept Chem, Tampa, FL 33620 USA Inst Nichtklass Chem eV, D-04318 Leipzig, Germany

Staudt, R.
论文数: 0 引用数: 0
h-index: 0
机构:
Inst Nichtklass Chem eV, D-04318 Leipzig, Germany Inst Nichtklass Chem eV, D-04318 Leipzig, Germany

Eddaoudi, M.
论文数: 0 引用数: 0
h-index: 0
机构:
Univ S Florida, Dept Chem, Tampa, FL 33620 USA Inst Nichtklass Chem eV, D-04318 Leipzig, Germany

Thommes, M.
论文数: 0 引用数: 0
h-index: 0
机构:
Quantachrome Instruments, Boynton Beach, FL USA Inst Nichtklass Chem eV, D-04318 Leipzig, Germany
[19]
Probing the adsorption sites for CO2 in metal organic frameworks materials MIL-53 (Al, Cr) and MIL-47 (V) by density functional theory
[J].
Ramsahye, N. A.
;
Maurin, G.
;
Bourrelly, S.
;
Llewellyn, P. L.
;
Serre, C.
;
Loiseau, T.
;
Devic, T.
;
Ferey, G.
.
JOURNAL OF PHYSICAL CHEMISTRY C,
2008, 112 (02)
:514-520

Ramsahye, N. A.
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Montpellier 2, CNRS, UMR 5253, ENSCM,UM2,Inst Charles Gerhardt Montpellier, F-34095 Montpellier 5, France Univ Montpellier 2, CNRS, UMR 5253, ENSCM,UM2,Inst Charles Gerhardt Montpellier, F-34095 Montpellier 5, France

Maurin, G.
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Montpellier 2, CNRS, UMR 5253, ENSCM,UM2,Inst Charles Gerhardt Montpellier, F-34095 Montpellier 5, France Univ Montpellier 2, CNRS, UMR 5253, ENSCM,UM2,Inst Charles Gerhardt Montpellier, F-34095 Montpellier 5, France

Bourrelly, S.
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Aix Marseille 1, Lab MADIREL, UMR 6121, CNRS, F-13397 Marseille 20, France Univ Montpellier 2, CNRS, UMR 5253, ENSCM,UM2,Inst Charles Gerhardt Montpellier, F-34095 Montpellier 5, France

Llewellyn, P. L.
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Aix Marseille 1, Lab MADIREL, UMR 6121, CNRS, F-13397 Marseille 20, France Univ Montpellier 2, CNRS, UMR 5253, ENSCM,UM2,Inst Charles Gerhardt Montpellier, F-34095 Montpellier 5, France

Serre, C.
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Versailles, CNRS, UMR 8180, Inst Lavoisier, F-78035 Versailles, France Univ Montpellier 2, CNRS, UMR 5253, ENSCM,UM2,Inst Charles Gerhardt Montpellier, F-34095 Montpellier 5, France

Loiseau, T.
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Versailles, CNRS, UMR 8180, Inst Lavoisier, F-78035 Versailles, France Univ Montpellier 2, CNRS, UMR 5253, ENSCM,UM2,Inst Charles Gerhardt Montpellier, F-34095 Montpellier 5, France

Devic, T.
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Versailles, CNRS, UMR 8180, Inst Lavoisier, F-78035 Versailles, France Univ Montpellier 2, CNRS, UMR 5253, ENSCM,UM2,Inst Charles Gerhardt Montpellier, F-34095 Montpellier 5, France

Ferey, G.
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Versailles, CNRS, UMR 8180, Inst Lavoisier, F-78035 Versailles, France Univ Montpellier 2, CNRS, UMR 5253, ENSCM,UM2,Inst Charles Gerhardt Montpellier, F-34095 Montpellier 5, France
[20]
Quasi-elastic neutron scattering and molecular dynamics study of methane diffusion in metal organic frameworks MIL-47(V) and MIL-53(Cr)
[J].
Rosenbach, Nilton, Jr.
;
Jobic, Herve
;
Ghoufi, Aziz
;
Salles, Fabrice
;
Maurin, Guillaume
;
Bourrelly, Sandrine
;
Llewellyn, Philip L.
;
Devic, Thomas
;
Serre, Christian
;
Ferey, Gerard
.
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION,
2008, 47 (35)
:6611-6615

Rosenbach, Nilton, Jr.
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Montpellier 2, Inst Charles Gerhardt Montpellier, F-34095 Montpellier 05, France Univ Lyon, Inst Rech Catalyse & Environm Lyon, CNRS, F-69626 Villeurbanne, France

Jobic, Herve
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Lyon, Inst Rech Catalyse & Environm Lyon, CNRS, F-69626 Villeurbanne, France Univ Lyon, Inst Rech Catalyse & Environm Lyon, CNRS, F-69626 Villeurbanne, France

Ghoufi, Aziz
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Montpellier 2, Inst Charles Gerhardt Montpellier, F-34095 Montpellier 05, France Univ Lyon, Inst Rech Catalyse & Environm Lyon, CNRS, F-69626 Villeurbanne, France

论文数: 引用数:
h-index:
机构:

Maurin, Guillaume
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Montpellier 2, Inst Charles Gerhardt Montpellier, F-34095 Montpellier 05, France Univ Lyon, Inst Rech Catalyse & Environm Lyon, CNRS, F-69626 Villeurbanne, France

Bourrelly, Sandrine
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Aix Marseille 1, Lab Chim Prov, Ctr St Jerome, CNRS,UMR 6264, F-13397 Marseille, France
Univ Aix Marseille 2, Lab Chim Prov, Ctr St Jerome, CNRS,UMR 6264, F-13397 Marseille, France
Univ Aix Marseille 3, Lab Chim Prov, Ctr St Jerome, CNRS,UMR 6264, F-13397 Marseille, France Univ Lyon, Inst Rech Catalyse & Environm Lyon, CNRS, F-69626 Villeurbanne, France

Llewellyn, Philip L.
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Aix Marseille 1, Lab Chim Prov, Ctr St Jerome, CNRS,UMR 6264, F-13397 Marseille, France
Univ Aix Marseille 2, Lab Chim Prov, Ctr St Jerome, CNRS,UMR 6264, F-13397 Marseille, France
Univ Aix Marseille 3, Lab Chim Prov, Ctr St Jerome, CNRS,UMR 6264, F-13397 Marseille, France Univ Lyon, Inst Rech Catalyse & Environm Lyon, CNRS, F-69626 Villeurbanne, France

Devic, Thomas
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Versailles, Inst Lavoisier, CNRS, UMR 8180, F-78035 Versailles, France Univ Lyon, Inst Rech Catalyse & Environm Lyon, CNRS, F-69626 Villeurbanne, France

Serre, Christian
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Versailles, Inst Lavoisier, CNRS, UMR 8180, F-78035 Versailles, France Univ Lyon, Inst Rech Catalyse & Environm Lyon, CNRS, F-69626 Villeurbanne, France

Ferey, Gerard
论文数: 0 引用数: 0
h-index: 0
机构:
Univ Versailles, Inst Lavoisier, CNRS, UMR 8180, F-78035 Versailles, France Univ Lyon, Inst Rech Catalyse & Environm Lyon, CNRS, F-69626 Villeurbanne, France