The effect of agitation states on hydrothermal synthesis of Bi2S3 nanorods

被引：46

作者：

Shao, MW ^{[1
]}

Mo, MS ^{[1
]}

Cui, Y ^{[1
]}

Chen, G ^{[1
]}

Qian, YT ^{[1
]}

机构：

[1] Univ Sci & Technol China, Dept Chem, Hefei 230026, Anhui, Peoples R China

来源：

JOURNAL OF CRYSTAL GROWTH | 2001年 / 233卷 / 04期

基金：

中国国家自然科学基金;

关键词：

crystallites; low dimensional structures; stirring; bismuth compounds; nanomaterials; sulfides;

D O I：

10.1016/S0022-0248(01)01649-9

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The effect of agitation states on the synthesis of Bi2S3 was discussed via stirred-assisted, oscillated-assisted and static hydrothermal preparation methods. Results showed that agitation influences the crystallinity and size of Bi2S3 nanorods. It is of interest that Bi2S3 nanorods with a high degree of crystallinity are obtained via stirred-assisted hydrothermal method at the temperature as low as 95 degreesC. (C) 2001 Elsevier Science B.V. All rights reserved.

引用

页码：799 / 802

页数：4

共 24 条

[1] SYNTHESIS OF D TRANSITION-METAL SULFIDES FROM AMORPHOUS DITHIOOXAMIDE COMPLEXES [J].

ABBOUDI, M ;

MOSSET, A .

JOURNAL OF SOLID STATE CHEMISTRY, 1994, 109 (01) :70-73

[2] Nanosize rutile titania particle synthesis via a hydrothermal method without mineralizers [J].

Aruna, ST ;

Tirosh, S ;

Zaban, A .

JOURNAL OF MATERIALS CHEMISTRY, 2000, 10 (10) :2388-2391

[3] ELECTRICAL AND OPTICAL PROPERTIES OF SOME M2V-BN3VI-B SEMICONDUCTORS [J].

BLACK, J ;

CONWELL, EM ;

SEIGLE, L ;

SPENCER, CW .

JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 1957, 2 (03) :240-251

[4] SYNTHESES OF NI3S2, CO9S8, AND ZNS BY THE DECOMPOSITION OF DIETHYLDITHIOCARBAMATE COMPLEXES [J].

CUI, H ;

PIKE, RD ;

KERSHAW, R ;

DWIGHT, K ;

WOLD, A .

JOURNAL OF SOLID STATE CHEMISTRY, 1992, 101 (01) :115-118

[5]

DESAI JD, 1993, INDIAN J PURE AP PHY, V31, P152

[6] STUDY AND DEVELOPMENT OF A GENERIC ELECTROCHEMICAL ION-EXCHANGE PROCESS TO FORM MXS OPTOELECTRONIC MATERIALS FROM ZNS PRECURSOR FILMS FORMED BY CHEMICAL-PRECIPITATION SOLUTION DEPOSITION [J].

ENGELKEN, RD ;

ALI, S ;

CHANG, LN ;

BRINKLEY, C ;

TURNER, K ;

HESTER, C .

MATERIALS LETTERS, 1990, 10 (06) :264-274

[7] BISMUTH(III) THIOLATES - SYNTHESES AND THE STRUCTURES OF A NEUTRAL THIOLATE AND A THIOLATO ANION [J].

FARRUGIA, LJ ;

LAWLOR, FJ ;

NORMAN, NC .

POLYHEDRON, 1995, 14 (02) :311-314

[8] OPTICAL-PROPERTIES OF AMORPHOUS AND CRYSTALLINE SB2S3 THIN-FILMS [J].

GHOSH, C ;

VARMA, BP .

THIN SOLID FILMS, 1979, 60 (01) :61-65

[9] Synthesis of zeolite MCM-22 under rotating and static conditions [J].

Güray, I ;

Warzywoda, J ;

Baç, N ;

Sacco, A .

MICROPOROUS AND MESOPOROUS MATERIALS, 1999, 31 (03) :241-251

[10] Chemical deposition of Bi2S3 thin films on glass substrates pretreated with organosilanes [J].

Huang, L ;

Nair, PK ;

Nair, MTS ;

Zingaro, RA ;

Meyers, EA .

THIN SOLID FILMS, 1995, 268 (1-2) :49-56

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