Determination of salbutamol and detection of other β-agonists in human postmortem whole blood and urine by GC-MS-SIM

被引:19
作者
Black, SB [1 ]
Hansson, RC [1 ]
机构
[1] Chem Ctr WA, Forens Sci Lab, E Perth, WA 6004, Australia
关键词
D O I
10.1093/jat/23.2.113
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
This paper details a sensitive and quantitative method for the determination of salbutamol and the detection of terbutaline, clenbuterol, fenoterol, and isoprenaline in postmortem human whole blood and urine. It describes solid-phase extraction using a XtrackT XRDAH515 column, formation of trimethylsilyl derivatives, and analysis by gas chromatography-mass spectrometry-selective ion monitoring.
引用
收藏
页码:113 / 118
页数:6
相关论文
共 34 条
[1]   RADIOIMMUNOASSAY FOR ALBUTEROL USING A MONOCLONAL-ANTIBODY - APPLICATION FOR DIRECT QUANTIFICATION IN HORSE URINE [J].
ADAM, A ;
ONG, H ;
SONDAG, D ;
RAPAILLE, A ;
MARLEAU, S ;
BELLEMARE, M ;
RAYMOND, P ;
GIROUX, D ;
LOO, JK ;
BEAULIEU, N .
JOURNAL OF IMMUNOASSAY, 1990, 11 (03) :329-345
[2]   DETERMINATION OF ALBUTEROL CONCENTRATIONS IN HUMAN PLASMA USING SOLID-PHASE EXTRACTION AND HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY WITH FLUORESCENCE DETECTION [J].
BLAND, RE ;
TANNER, RJN ;
CHERN, WH ;
LANG, JR ;
POWELL, JR .
JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 1990, 8 (07) :591-596
[3]   THERMOSPRAY LIQUID-CHROMATOGRAPHY MASS-SPECTROMETRY FOR THE CHARACTERIZATION OF SULFATE ESTER CONJUGATES [J].
BOWERS, GD ;
HIGTON, DM ;
MANCHEE, GR ;
OXFORD, J ;
SAYNOR, DA .
JOURNAL OF CHROMATOGRAPHY, 1991, 554 (1-2) :175-180
[4]   DETERMINATION OF SALBUTAMOL IN HUMAN-PLASMA AND URINE BY HIGH-PERFORMANCE THIN-LAYER CHROMATOGRAPHY [J].
COLTHUP, PV ;
DALLAS, FAA ;
SAYNOR, DA ;
CAREY, PF ;
SKIDMORE, LF ;
MARTIN, LE ;
WILSON, K .
JOURNAL OF CHROMATOGRAPHY, 1985, 345 (01) :111-118
[5]   HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC DETERMINATION OF CLENBUTEROL AND CIMATEROL USING POSTCOLUMN DERIVATIZATION [J].
COURTHEYN, D ;
DESAEVER, C ;
VERHE, R .
JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS, 1991, 564 (02) :537-549
[6]   DETERMINATION OF BETA-AGONIST RESIDUES IN HUMAN PLASMA USING LIQUID-CHROMATOGRAPHY ATMOSPHERIC-PRESSURE CHEMICAL-IONIZATION MASS-SPECTROMETRY AND TANDEM MASS-SPECTROMETRY [J].
DOERGE, DR ;
BAJIC, S ;
BLANKENSHIP, LR ;
PREECE, SW ;
CHURCHWELL, MI .
JOURNAL OF MASS SPECTROMETRY, 1995, 30 (06) :911-916
[7]   SCREENING AND CONFIRMATORY ANALYSIS OF BETA-AGONISTS, BETA-ANTAGONISTS AND THEIR METABOLITES IN HORSE URINE BY CAPILLARY GAS-CHROMATOGRAPHY MASS-SPECTROMETRY [J].
DUMASIA, MC ;
HOUGHTON, E .
JOURNAL OF CHROMATOGRAPHY-BIOMEDICAL APPLICATIONS, 1991, 564 (02) :503-513
[8]  
Garcia Regueiro J. A., 1993, Journal of Chromatography A, V655, P73, DOI 10.1016/0021-9673(93)87012-B
[9]   DETERMINATION OF CLENBUTEROL IN BOVINE PLASMA AND TISSUES BY GAS-CHROMATOGRAPHY NEGATIVE-ION CHEMICAL IONIZATION MASS-SPECTROMETRY [J].
GIRAULT, J ;
FOURTILLAN, JB .
JOURNAL OF CHROMATOGRAPHY, 1990, 518 (01) :41-52
[10]   QUANTITATIVE MEASUREMENT OF CLENBUTEROL AT THE FEMTOMOLE LEVEL IN PLASMA AND URINE BY COMBINED GAS-CHROMATOGRAPHY NEGATIVE-ION CHEMICAL IONIZATION MASS-SPECTROMETRY [J].
GIRAULT, J ;
GOBIN, P ;
FOURTILLAN, JB .
BIOMEDICAL AND ENVIRONMENTAL MASS SPECTROMETRY, 1990, 19 (02) :80-88