Early results from an aberration-corrected JEOL 2200FS STEM/TEM at Oak Ridge National Laboratory

被引:24
作者
Blom, Douglas A.
Allard, Lawrence F.
Mishina, Satoshi
O'Keefe, Michael A.
机构
[1] Oak Ridge Natl Lab, Div Mat Sci & Technol, Oak Ridge, TN 37831 USA
[2] JEOL USA, Peabody, MA 01960 USA
[3] Univ Calif Berkeley, Lawrence Berkeley Lab, Div Mat Sci, Berkeley, CA 94720 USA
关键词
aberration-corrected scanning transmission electron microscopy; high-angle annular dark-field imaging; single atom imaging; atomic resolution;
D O I
10.1017/S1431927606060570
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The resolution-limiting aberrations of round electromagnetic lenses can now be successfully overcome via the use of multipole element "aberration correctors." The installation and performance of a hexapole-based corrector (CEOS GmbH) integrated on the probe-forming side of a JEOL 2200FS FEG STEM/TEM is described. For the resolution of the microscope not to be severely compromised by its environment, a new, specially designed building at Oak Ridge National Laboratory has been built. The Advanced Microscopy Laboratory was designed with the goal of providing a suitable location for aberration-corrected electron microscopes. Construction methods and performance of the building are discussed in the context of the performance of the microscope. Initial performance of the microscope on relevant specimens and modifications made to eliminate resolution-limiting conditions are also discussed.
引用
收藏
页码:483 / 491
页数:9
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