MoS2: Preparation and their characterization

被引:78
作者
Garadkar, K. M. [1 ]
Patil, A. A. [1 ]
Hankare, P. P. [1 ]
Chate, P. A. [2 ]
Sathe, D. J. [1 ]
Delekar, S. D. [3 ]
机构
[1] Shivaji Univ, Dept Chem, Mat Sci Res Lab, Kolhapur 416004, Maharashtra, India
[2] JSM Coll, Dept Chem, Alibag, Maharashtra, India
[3] Dr BAM Univ, PG Sub Ctr, Osmanabad, Maharashtra, India
关键词
Thin films; Optical properties; X-ray diffraction; CHEMICAL BATH DEPOSITION; THIN-FILMS; SYNTHETIC ROUTE; SOLAR-CELLS; PERFORMANCE;
D O I
10.1016/j.jallcom.2009.08.069
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Molybdenum disulphide thin films were deposited using chemical bath deposition method on non-conducting glass substrate using tartaric acid as a complexing agent at 363 K. The films were characterized by X-ray diffraction, scanning electron microscopy, optical absorption and electrical measurements. X-ray diffraction pattern shows that polycrystalline with hexagonal structure. The direct optical band gap was found to be 1.8 eV. Electrical measurement suggests that specific conductance was found in the order of 10(-5) to 10(-2) (Omega cm)(-1) and showing n-type conduction mechanism. (C) 2009 Elsevier B.V. All rights reserved.
引用
收藏
页码:786 / 789
页数:4
相关论文
共 27 条
[1]   A study of textured non-stoichiometric MoTe2 thin films used as substrates for textured stoichlometric MoS2 thin films [J].
Amory, C ;
Bernède, JC ;
Hamdadou, N .
VACUUM, 2004, 72 (04) :351-361
[2]  
Bucher E., 1992, PHOTOELECTROCHEMISTY, P36
[3]  
Chopra K.L., 1969, THIN FILM PHENOMENON
[4]   Pulsed electrodeposition and characterization of molybdenum diselenide thin film [J].
Delphine, SM ;
Jayachandran, M ;
Sanjeeviraja, C .
MATERIALS RESEARCH BULLETIN, 2005, 40 (01) :135-147
[5]   SEMICONDUCTOR ELECTRODES .29. HIGH-EFFICIENCY PHOTOELECTROCHEMICAL SOLAR-CELLS WITH N-WSE2 ELECTRODES IN AN AQUEOUS IODIDE MEDIUM [J].
FAN, FRF ;
WHITE, HS ;
WHEELER, B ;
BARD, AJ .
JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 1980, 127 (02) :518-520
[6]   FUNDAMENTAL-ASPECTS OF THE ELECTRONIC-STRUCTURE, MATERIALS PROPERTIES AND LUBRICATION PERFORMANCE OF SPUTTERED MOS2 FILMS [J].
FLEISCHAUER, PD .
THIN SOLID FILMS, 1987, 154 (1-2) :309-322
[7]   Kinetics of the chemical bath deposition of ZnSe films [J].
Ganchev, M ;
Stratieva, N ;
Tzvetkova, E ;
Gadjov, I .
JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS, 2003, 14 (10-12) :847-848
[8]   Novel chemical synthetic route and characterization of zinc selenide thin films [J].
Hankare, P. P. ;
Chate, P. A. ;
Delekar, S. D. ;
Asabe, M. R. ;
Mulla, I. S. .
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 2006, 67 (11) :2310-2315
[9]   Characterization of MoSe2 thin film deposited at room temperature from solution phase [J].
Hankare, P. P. ;
Patil, A. A. ;
Chate, P. A. ;
Garadkar, K. M. ;
Sathe, D. J. ;
Manikshete, A. H. ;
Mulla, I. S. .
JOURNAL OF CRYSTAL GROWTH, 2008, 311 (01) :15-19
[10]   Novel chemical synthetic route and characterization of tungsten diselenide thin films [J].
Hankare, P. P. ;
Manikshete, A. H. ;
Sathe, D. J. ;
Chate, P. A. ;
Rathod, K. C. .
MATERIALS CHEMISTRY AND PHYSICS, 2009, 113 (01) :183-186