THE 900-DEGREES-C UPPER YIELD STRESS OF CZOCHRALSKI SILICON SINGLE-CRYSTALS WITH CARBON CONCENTRATIONS OF 4.0X10(14) AND 3.5X10(15) CM(-3)

被引:9
作者
FUKUDA, T
KOIZUKA, M
机构
[1] Semiconductor Devices Laboratory, Fujitsu Laboratories Ltd., Atsugi 243-01
关键词
D O I
10.1063/1.354677
中图分类号
O59 [应用物理学];
学科分类号
摘要
In order to investigate the influence of carbon on the high-temperature strength of Czochralski silicon single crystals, we measured the 900-degrees-C upper yield stress of crystals containing carbon at concentrations of 4.0 X 10(14) cm-3 (''low C'') and 3.5 X 10(15) cm-3 (''standard C''). Prior to testing, all crystals were beat treated for 20 h at 700-degrees-C. They were then annealed at 1000-degrees-C for periods between 1.5-7 h. During the longest anneal, the interstitial oxygen content fell from 2.0 X 10(18) to 1.0 X 10(18) cm-3 in low C crystals and from 1.9 X 10(18) to 7 X 10(17) cm-3 in ''standard C'' crystals. The 900-degrees-C upper yield stress of 7 h annealed low C crystals is 13 MPa, which is 30-40% higher than that measured in standard C crystals. The precipitate density, measured optically, is 4 X 10(5) cm-2 in low C samples and 9 X 10(5) cm-2 in standard C crystals. In all cases, the precipitates punched out dislocations. A model that assumes that the higher interstitial oxygen content retained by the low C crystals results in higher locking stresses for glide dislocations can quantitatively account for these observations.
引用
收藏
页码:2420 / 2424
页数:5
相关论文
共 22 条
[1]   DYNAMIC OXYGEN EQUILIBRIUM IN SILICON MELTS DURING CRYSTAL-GROWTH BY THE CZOCHRALSKI TECHNIQUE [J].
CARLBERG, T ;
KING, TB ;
WITT, AF .
JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 1982, 129 (01) :189-193
[2]   MECHANICAL STRENGTH OF CZOCHRALSKI SILICON-CRYSTALS WITH CARBON CONCENTRATIONS AT AND BELOW 10(15) CM(-3) [J].
FUKUDA, T ;
OHSAWA, A .
JOURNAL OF APPLIED PHYSICS, 1993, 73 (01) :112-117
[3]   ENHANCEMENT OF OXYGEN PRECIPITATION IN QUENCHED CZOCHRALSKI SILICON-CRYSTALS [J].
HARA, A ;
FUKUDA, T ;
MIYABO, T ;
HIRAI, I .
JOURNAL OF APPLIED PHYSICS, 1989, 66 (08) :3958-3960
[4]  
HARA A, 1992, 1992 INT C SOL STAT, P35
[5]   INDENTATION ROSETTES AND DISLOCATION LOCKING BY OXYGEN IN SILICON [J].
HARADA, H ;
SUMINO, K .
JOURNAL OF APPLIED PHYSICS, 1982, 53 (07) :4838-4842
[6]   DISLOCATION PINNING EFFECT OF OXYGEN-ATOMS IN SILICON [J].
HU, SM .
APPLIED PHYSICS LETTERS, 1977, 31 (02) :53-55
[7]   THERMALLY INDUCED MICRODEFECTS IN CZOCHRALSKI-GROWN SILICON - NUCLEATION AND GROWTH-BEHAVIOR [J].
KISHINO, S ;
MATSUSHITA, Y ;
KANAMORI, M ;
IIZUKA, T .
JAPANESE JOURNAL OF APPLIED PHYSICS PART 1-REGULAR PAPERS SHORT NOTES & REVIEW PAPERS, 1982, 21 (01) :1-12
[8]  
KISHINO S, 1980, OYO BUTSURI, V49
[9]  
LAWRENCE JD, 1986, MATER RES SOC S P, V59, P389
[10]   INFLUENCE OF CARBON ON OXYGEN BEHAVIOR IN SILICON [J].
LEROUEILLE, J .
PHYSICA STATUS SOLIDI A-APPLIED RESEARCH, 1981, 67 (01) :177-181